反応 #524769

反応方程式

isochroman-1,3-dione

N,N-bis-(3-amino-propyl)-amine

→

N,N-Bis-[3-(3,4-dihydro-1,3-dioxo-2(1H)-isoquinolyl)-propyl]-amine

反応条件

後処理

1. 1
   その他The hydrochloride was precipitated from acetone with ethereal hydrochloric acid
2. 2
   その他135° -140° C

実験手順

N,N-Bis-[3-(3,4-dihydro-1,3-dioxo-2(1H)-isoquinolyl)-propyl]-amine was prepared analogous to Example 30 from 2.44 gm of isochroman-1,3-dione and N,N-bis-(3-amino-propyl)-amine. The hydrochloride was precipitated from acetone with ethereal hydrochloric acid. M.p. of the hydrochloride: 135° -140° C; yield: 0.17 gm (2.5% of the theory).

出典