反応 #522335

ord-87f7f8fdccd942339b4b991bede3ba02

反応条件

温度
170°CELSIUS
詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他condensed at 85° C. for 10 hours in a reactor

実験手順

206 g (1 mole) of p-tert-octylphenol, 30 g (0.8 mole) of 80% paraformaldehyde and 6 g of oxalic acid dihydrate were condensed at 85° C. for 10 hours in a reactor. The reaction mixture was dehydrated by heating it to 170° C. to give a p-tert-octylphenol/formaldehyde condensate.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04400492uspto-grants-1983_08