反応 #5223

反応方程式

2-Aminoethanol

palmitoyl chloride

→

2-Palmitoylaminoethanol

溶媒

CHCl3

反応条件

後処理

1. 1
   workup.STIRRINGThereafter, the mixture was stirred at room temperature for 19 hours

実験手順

2-Aminoethanol (13.76 g, 225.3 mmol) was dissolved in CHCl3 (750 ml). To the solution was added dropwise palmitoyl chloride (15.48 g, 56.3 mmol) with stirring under ice cooling. Thereafter, the mixture was stirred at room temperature for 19 hours.

出典