反応 #52110
ord-c62d3ce4d7174d1fad0761d7168f165f
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1温度an attached reflux condenser
実験手順
2 mmol of N-hydroxyphthalimide and 4 mmol of cumene hydroperoxide are added at a temperature of 130° C. to 200 mmol of cyclooctane in a round-bottomed flask having an attached reflux condenser. Oxygen at approximately 15 l/h is passed through the reaction mixture for 8 hours at said temperature. Cyclooctanol is obtained at a selectivity of 17% and cyclooctanone at a selectivity of 46%, at a cyclooctcane conversion rate of 53%.