反応 #520070

反応方程式

compound ( 206 )

4-(α-methylbenzyloxy)-3-ethyl-3,5,5-trimethylmorpholin-2-one

t-butylperoxide

→

compound ( 210 )

収率 52.0%

4-(α-methylbenzyloxy)-3,3-diethyl-5,5-dimethylmorpholin-2-one

収率 52.0%

溶媒

ethylbenzene

反応条件

実験手順

In analogy to Example B3, compound (206), 4.75 g (0.026 mol) of 3,3-diethyl-5,5-dimethylmorpholin-2-on-4-oxyl are reacted with t-butylperoxide and ethylbenzene as solvent, resulting in 4.1 g (52%) of compound (210) in the form of a colourless oil.

出典