反応 #51463

反応方程式

N-Boc sarcosine piperonylamide

acetyl chloride

→

sarcosine piperonyl amide hydrochloride

溶媒

methanol

反応条件

後処理

1. 1
   その他all volatiles were removed under reduced pressure

実験手順

N-Boc sarcosine piperonylamide (500 mg, 1.54 mmol) in methanol (10 mL) was treated with acetyl chloride (1 mL). After 45 minutes, all volatiles were removed under reduced pressure to yield sarcosine piperonyl amide hydrochloride (395 mg, quant.) as a sticky solid.

出典