反応 #514222

反応方程式

Methyl 3-(2-aminoanilino)-2,5-dihydrothiophene-4-carboxylate

norbornadiene

norbornylene

→

Methyl 3-(2-aminoanilino)-thiophene-4-carboxylate

溶媒

cyclohexene

反応条件

後処理

1. 1
   温度the reaction was heated
2. 2
   温度at reflux

実験手順

Methyl 3-(2-aminoanilino)-2,5-dihydrothiophene-4-carboxylate (2.5 g, 0.001 mol) was added to a flask containing palladium on charcoal catalyst (5%, 200 mg) in cyclohexene (or norbornadiene or norbornylene) (50 ml and the reaction was heated at reflux with stirring for 4 hours, the reaction being followed by t.l.c.

出典