反応 #51346

反応方程式

3,4-dichlorophenylacetic acid

L-alanine iso-butyl ester hydrochloride

→

title compound

N-[(3,4-dichlorophenyl)acetyl]-L-alanine iso-butyl ester

反応条件

後処理

1. 1
   その他The reaction was monitored by tlc on silica gel and purification
2. 2
   抽出was by extraction with Et2O

実験手順

Following General Procedure BB and using 3,4-dichlorophenylacetic acid (Aldrich) and L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared as a solid having a melting point of 81°-83° C. The reaction was monitored by tlc on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.

出典