反応 #51330

ord-e4defc8176564c78905f4f164eeb6e1d

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他Purification

実験手順

Following General Procedure AA above and using 6-amino-2-methylquinoline (Lancaster) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared. The reaction was monitored by silica gel tlc (Rf=0.44 in 50% EtOAc/hexanes). Purification was by flash chromatography (silica gel using 50% EtOAc/hexanes as the eluant).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06849650B2uspto-grants-2005_02