反応 #50163
ord-0aba0da7a8164d719a0f863898cfe358
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1温度the mixture was heated
- 2温度to reflux for 12 hours
実験手順
A solution of hexamethylenetretramine (1.87 mmol, 0.27 g) in trifluoroacetic acid (1.4 cm3) was added to benzo 15-crown-5 ether (1.87 mmol, 0.5 g) under nitrogen; the mixture was heated to reflux for 12 hours.