反応 #501579

反応方程式

naphthacene-5-carbaldehyde

Naphthacene-5-carbaldehyde

2-amino-2-methyl-1,3-propanediol

→

2-[(5-naphthacenylmethyl)amino]-2-methyl-1,3-propanediol

収率 50.1%

溶媒

EtOH Et2O

反応条件

実験手順

Using the reductive amination procedure described in Example 1, naphthacene-5-carbaldehyde (3A) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave 50.1% yield of 2-[(5-naphthacenylmethyl)amino]-2-methyl-1,3-propanediol methanesulfonte, mp 197.5°-199°, (EtOH/Et2O), (C, H, N, S).

出典