反応 #501292

ord-4b447846255647969ae905571ab14d0c

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The same isocyanuration reaction as in Example 1

実験手順

The same isocyanuration reaction as in Example 1 was carried out except that 3,290 g of hexamethylene diisocyanate and 210 g of "Takenate 500" (xylylene diisocyanate produced by Takeda Chemical Industry Co., Ltd.) were used instead of 3,500 g of hexamethylene diisocyanate, and the amount of the isocyanuration catalyst used in Example 1 was changed to 4.7 g. There was obtained 4,219 g of the reaction mixture containing the deactivated catalyst.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04789705uspto-grants-1988_12