反応 #5007

反応方程式

2-methylbenzyl bromide

triisopropyl phosphite

→

diisopropyl 2-methylbenzylphosphonate

反応条件

後処理

1. 1
   workup.DISTILLATIONDuring this procedure, i-propyl bromide distilled off
2. 2
   workup.DISTILLATIONThe product was distilled through a 30 cm Vigreux column

実験手順

34.5 g (0.19 mol) of 2-methylbenzyl bromide and 39 g (0.19 mol) of triisopropyl phosphite were heated at 150° C. for 2 hours. During this procedure, i-propyl bromide distilled off. The product was distilled through a 30 cm Vigreux column.

出典