反応 #49707

反応方程式

4'-n-octylbiphenyl-4-carboxylic acid

thionyl chloride

→

4'-n-octylbiphenyl-4-carboxylic acid chloride

反応条件

後処理

1. 1
   温度under refluxing for 6 hours
2. 2
   workup.DISTILLATIONunaltered thionyl chloride was distilled off

実験手順

After 4'-n-octylbiphenyl-4-carboxylic acid (3.2 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours, unaltered thionyl chloride was distilled off to obtain 4'-n-octylbiphenyl-4-carboxylic acid chloride.

出典