反応 #47736
ord-b51d7cb6b41e41718e3f39d76b7da4bc
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他was evaporated under reduced pressure
実験手順
Glutaric anhydride (215 mg, 1.9 mmol) was dissolved in anhydrous dichloromethane (7 ml) and followed by the addition of 3-ethynylaniline (200 mg, 1.7 mmol). The mixture was allowed to stir at room temperature for 6 hours before the solvent was evaporated under reduced pressure to provide the product as a white solid (363 mg, 99%);