反応 #4730

ord-0b658159483d4944933cf94782ffab90

反応方程式

CC(C)NC(=O)NNC(=O)NCCCOc1cccc(CN2CCCCC2)c1
N-isopropyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride
→
CC(C)Nc1nnc(NCCCOc2cccc(CN3CCCCC3)c2)o1
N-Isopropyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]1,3,4-oxadiazole-2,5-diamine

反応物

CC(C)NC(=O)NNC(=O)NCCCOc1cccc(CN2CCCCC2)c1
N-isopropyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The compound is prepared by a method analogous to that of Example 40 from N-isopropyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide and phosphorus oxychloride. The analytical values are summarized in Table III.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04727081uspto-grants-1988_02