反応 #470412

反応方程式

4′,7-Dihydroxyisoflav-3-ene

ethanol

Propylamine

formaldehyde

→

title compound

収率 53.0%

4-(3-Propyl-2,3,4,8-tetrahydrochromeno[6,7-e][1,3]oxazin-7-yl)phenol

収率 53.0%

反応条件

後処理

1. 1
   その他The white precipitate was collected

実験手順

4′,7-Dihydroxyisoflav-3-ene (503 mg, 2.09 mmol) was dissolved in ethanol (20 ml). Propylamine (0.25 ml, 3.04 mmol) was added followed by formaldehyde solution (2 ml, 0.03 mol, 37% wt.). The reaction was stirred at room temperature for 1 day. The white precipitate was collected to afford the title compound (362 mg, 53%).

出典