反応 #470372

反応方程式

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methoxymethyl-N-Methylpyrrolidinium Chloride

lithium bis(pentafluoroethanesulfonyl)imide

dichloromethane

→

colorless liquid

N-Methoxymethyl-N-Methylpyrrolidinium bis(pentafluoroethanesulfonyl)imide

溶媒

water

反応条件

後処理

1. 1
   抽出followed by extraction
2. 2
   洗浄The organic layer was washed with 50 g of water ten times
3. 3
   その他dried

実験手順

A 15.0 g quantity of N-methoxymethyl-N-methylpyrrolidinium chloride prepared in Example 10 was dissolved in 50 g of water, and 35.1 g of lithium bis(pentafluoroethanesulfonyl)imide was added to the solution. The mixture was stirred for 30 minutes, and dichloromethane was thereafter added to the mixture, followed by extraction. The organic layer was washed with 50 g of water ten times and then dried, giving 31.4 g of a colorless liquid as the desired product.

出典