反応 #470371

反応方程式

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methoxymethyl-N-Methylpyrrolidinium Chloride

potassium hexafluorophosphate

→

white solid

N-Methoxymethyl-N-Methylpyrrolidinium hexafluorophosphate

溶媒

water

反応条件

後処理

1. 1
   その他separated out
2. 2
   workup.ADDITIONdichloromethane was thereafter added to the mixture for extraction
3. 3
   洗浄The organic layer was washed with 120 g of water six times
4. 4
   その他dried

実験手順

A 20.0 g quantity of N-methoxymethyl-N-methylpyrrolidinium chloride prepared in Example 10 was dissolved in 120 g of water, and 22.2 g of potassium hexafluorophosphate was added to the solution, whereupon a white solid separated out. The mixture was stirred for 30 minutes, and dichloromethane was thereafter added to the mixture for extraction. The organic layer was washed with 120 g of water six times and then dried, affording 25.1 g of a white solid as the desired product.

出典