反応 #470370

反応方程式

sodium trifluoroacetate

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methyl-N-Methoxymethylpyrrolidinium Chloride

→

colorless liquid

N-Methoxymethyl-N-Methylpyrrolidinium trifluoroacetate

溶媒

methanol

反応条件

後処理

1. 1
   濃縮concentrated in a vacuum
2. 2
   その他dried in a vacuum
3. 3
   workup.DISSOLUTIONThe residue was dissolved in 500 ml of dichloromethane
4. 4
   ろ過followed by filtration with a membrane
5. 5
   ろ過filter
6. 6
   濃縮concentration in a vacuum
7. 7
   その他drying

実験手順

A 14.94 g quantity of sodium trifluoroacetate was dissolved in 100 g of methanol, and 18.20 g of N-methoxymethyl-N-methylpyrrolidinium chloride was added to the solution at room temperature. The mixture was stirred for 1 hour, concentrated in a vacuum and dried in a vacuum using a vacuum pump. The residue was dissolved in 500 ml of dichloromethane, followed by filtration with a membrane filter, concentration in a vacuum and drying, affording 26.52 g of a colorless liquid as the desired product.

出典