反応 #470367

反応方程式

Methoxymethylpyrrolidine

dimethyl carbonate

→

desired product

収率 60.0%

N-Methoxymethyl-N-Methylpyrrolidinium Methyl carbonate

収率 60.0%

反応条件

後処理

1. 1
   その他reacted at 120° C. for 24 hours
2. 2
   ろ過The resulting solids were filtered off
3. 3
   洗浄washed with dimethyl carbonate
4. 4
   その他The solids were dried in a vacuum

実験手順

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

出典