反応 #466690

ord-d2912ed95edd4b108b23c3a7feb1bdf4

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The hydrate lead acetate is dissolved in butoxyethanol (BuEtOH) (1) at 60° C. The resulting solution is kept at this temperature for two hours, and is cooled down slowly (2) to thereby form a precipitate of dehydrated lead acetate. The precipitation yield can be promoted by further cooling down the vessel containing said solution in an ice bath.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06300144B1uspto-grants-2001_10