反応 #465935

ord-02c47444813f491eb7b99c1d7a363f28

反応方程式

COc1ccccc1OC
1,2-dimethoxy benzene
O=C(Cl)c1ccccc1
benzoyl chloride
[Al+3].[Cl-].[Cl-].[Cl-]
aluminum chloride
COc1ccc(C(=O)c2ccccc2)cc1OC
3,4-dimethoxy benzophenone
収率 95.7%

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The process of Step 1, Example 4 was followed except that 292 grams of 1,2-dimethoxy benzene, 297 grams of benzoyl chloride, and 281 grams of aluminum chloride were used to yield 490 grams of 3,4-dimethoxy benzophenone.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06296785B1uspto-grants-2001_10