反応 #458534

ord-ba8f55358b724aae850948f997db5f29

反応方程式

O=C(Nc1cc([N+](=O)[O-])c2c([N+](=O)[O-])c(NC(=O)C(F)(F)F)cc([N+](=O)[O-])c2c1[N+](=O)[O-])C(F)(F)F
2,6-di(trifluoroacetamido)-1,4,5,8-tetranitronaphthalene
Cl
hydrogen chloride
→
Nc1cc([N+](=O)[O-])c2c([N+](=O)[O-])c(N)cc([N+](=O)[O-])c2c1[N+](=O)[O-]
2,6-diamino-1,4,5,8-tetranitronaphthalene

反応物

O=C(Nc1cc([N+](=O)[O-])c2c([N+](=O)[O-])c(NC(=O)C(F)(F)F)cc([N+](=O)[O-])c2c1[N+](=O)[O-])C(F)(F)F
2,6-di(trifluoroacetamido)-1,4,5,8-tetranitronaphthalene
Cl
hydrogen chloride

試薬

なし

溶媒

CO
methanol

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

reacting said 2,6-di(trifluoroacetamido)-1,4,5,8-tetranitronaphthalene with methanol and dry hydrogen chloride to form 2,6-diamino-1,4,5,8-tetranitronaphthalene.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04531013uspto-grants-1985_07