反応 #452433

反応方程式

4-dimethylamino-1-cyclohexanone ethylene ketal

→

title compound

収率 100.0%

4-dimethylamino-1-cyclohexanone

収率 100.0%

溶媒

formic acid

反応条件

後処理

1. 1
   温度at reflux for 18 hours
2. 2
   温度The reaction mixture was then cooled to ambient and the volatiles
3. 3
   その他removed under reduced pressure

実験手順

4.96 gm (26.8 mMol) 4-dimethylamino-1-cyclohexanone ethylene ketal were dissolved in 50 mL formic acid and the solution stirred at reflux for 18 hours. The reaction mixture was then cooled to ambient and the volatiles removed under reduced pressure to give 3.78 gm (100%) of the title compound.

出典