反応 #452430
ord-8ae4c1cbb2f44f23852ec10903d48b5b
反応方程式
o-chlorophenyl-acetic acid
thionyl chloride
→
o-chloro-phenylacetyl chloride
収率 99.0%
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他The volatiles were then removed in vacuo
実験手順
A mixture of 30.0 gm (0.176 mole) of o-chlorophenyl-acetic acid and 40.0 mL of thionyl chloride was stirred at ambient temperature for 18 hours. The volatiles were then removed in vacuo to give 32.76 gm (99.0 %) of o-chloro-phenylacetyl chloride as a transparent, pale yellow, mobile liquid.