反応 #45225

反応方程式

3-(3-amino-phenyl)-acrylic acid methyl ester

→

3-(3-amino-phenyl)propionic acid methyl ester

収率 98.9%

溶媒

ethanol

反応条件

後処理

1. 1
   ろ過filtered over Celite
2. 2
   その他Removal of the volatiles in vacuo

実験手順

A mixture of 3-(3-amino-phenyl)-acrylic acid methyl ester (6 g) and 10% Pd on activated carbon (1 g) in ethanol (50 ml) was hydrogenated at 30 psi for 18 h and filtered over Celite. Removal of the volatiles in vacuo provided 3-(3-amino-phenyl)propionic acid methyl ester (6 g).

出典