反応 #44839

ord-dad6b99b1e534901ae53ca3c06261cc2

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The title compound was prepared from 4,5-dimethylphenylenediamine and (R)-l-isothiocyanato-1,2,3,4-tetrahydronaphthalene by Procedure D. The title compound was isolated by column chromatography as the free base (solid, mp 121-124° C.). MS(ES+) m/z 292 ([M+1]+, 100).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07737167B2uspto-grants-2010_06