反応 #445377
ord-31e0f680e83a4e5bbd90c0566663e97b
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Methyl 5-fluoro-2-nitrobenzoate was reacted with the sodium salt of 4-chloro-3-methylphenol (prepared from sodium hydride and the phenol) in dimethylformamide at 100° C. for 2.5 hours and the resulting methyl 5(4-chloro-3-methylphenoxy)-2-nitrobenzoate isolated in the usual way; the ester had a melting point of 85°-87° C.