反応 #44484

ord-272aeb37cfe24c39bb51f81365c79ccf

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The solvent was evaporated in vacuo

実験手順

Two drops of 12M HCl was added to a solution of Example 1D (75 mg, 0.21 mmoles) in methanol (1.25 mL) and stirred for one hour at room temperature. The solvent was evaporated in vacuo to provide the title compound as a colorless oil.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07737137B2uspto-grants-2010_06