反応 #443208

ord-fa896edfe4b34c0fa74014413e3506a2

反応方程式

Clc1cc2cc[nH]c2cc1Cl
5,6-Dichloroindole
[BH3-]C#N.[Na+]
sodium cyanoborohydride
Clc1cc2c(cc1Cl)NCC2
title compound ( D39 )
収率 90.0%
Clc1cc2c(cc1Cl)NCC2
5,6-Dichloroindoline
収率 90.0%

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

5,6-Dichloroindole (D38) was reduced in the usual way with sodium cyanoborohydride in glacial acetic acid to give the title compound (D39) (1.18 g, 90%).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05834494uspto-grants-1998_11