反応 #433598

反応方程式

3,4-Dichloro-6-fluoroaniline

4-chloro-7-fluoro-6-nitroquinazoline

→

4-[(3,4-dichloro-6-fluorophenyl)amino]-7-fluoro-6-nitroquinazoline

収率 78.0%

溶媒

iso-propylalcohol

反応条件

後処理

1. 1
   ろ過After filtration

実験手順

3,4-Dichloro-6-fluoroaniline (1 equivalent) was reacted with 4-chloro-7-fluoro-6-nitroquinazoline (3.5 equivalents), in iso-propylalcohol. After filtration, 4-[(3,4-dichloro-6-fluorophenyl)amino]-7-fluoro-6-nitroquinazoline was obtained in 78% yield.

出典