反応 #432364

反応方程式

2,5-Dimercapto-1,3,4-thiadiazole

dibutyl maleate

→

2,5-Bis(1,2-di(butoxycarbonyl)ethylthio)-1,3,4-thiadiazole

反応条件

後処理

1. 1
   ろ過The reaction product was filtered
2. 2
   温度warm
3. 3
   ろ過using filter aid

実験手順

2,5-Dimercapto-1,3,4-thiadiazole (50.09 g, 0.33 mol) and dibutyl maleate (157.0 g, 0.69 mol) were charged in a reaction flask and heated to 55° C. for 4 hours. The reaction product was filtered warm using filter aid.

出典