反応 #4296

ord-fb82c5ce9e9d4fb38a0048e765370c2d

反応方程式

CC(C)N(CCS(=O)(=O)c1ccc(Cl)cc1)C(=O)Oc1ccccc1
N-[2-[(4-chlorophenyl)sulfonyl]ethyl]-N-(1-methylethyl)carbamic acid phenyl ester
CC(C)N(CCS(=O)(=O)c1ccc(Cl)c(Cl)c1)C(=O)Oc1ccccc1
N-[2-[(3,4-dichlorophenyl)sulfonyl]ethyl]-N-(1-methylethyl)carbamic acid phenyl ester
→
CC(C)NCCS(=O)(=O)c1ccc(Cl)cc1.Cl
title compound
CC(C)NCCS(=O)(=O)c1ccc(Cl)cc1.Cl
N-[2-[(4-Chlorophenyl)sulfonyl]ethyl]-1-methylethanamine hydrochloride

反応物

CC(C)N(CCS(=O)(=O)c1ccc(Cl)cc1)C(=O)Oc1ccccc1
N-[2-[(4-chlorophenyl)sulfonyl]ethyl]-N-(1-methylethyl)carbamic acid phenyl ester
CC(C)N(CCS(=O)(=O)c1ccc(Cl)c(Cl)c1)C(=O)Oc1ccccc1
N-[2-[(3,4-dichlorophenyl)sulfonyl]ethyl]-N-(1-methylethyl)carbamic acid phenyl ester

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

When in the procedure of Preparation 29, N-[2-[(4-chlorophenyl)sulfonyl]ethyl]-N-(1-methylethyl)carbamic acid phenyl ester is substituted for N-[2-[(3,4-dichlorophenyl)sulfonyl]ethyl]-N-(1-methylethyl)carbamic acid phenyl ester, the title compound is obtained.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04724235uspto-grants-1988_02