反応 #4256

反応方程式

oleylamine

styrene oxide

toluene

boron

→

oleylamine styrene oxide

溶媒

water

反応条件

後処理

1. 1
   温度cooled condenser
2. 2
   温度The mixture is heated
3. 3
   温度under reflux for three hours

実験手順

A sulfurized, boron-containing, heterocyclic compound is prepared by mixing 12 grams of oleylamine, 9.6 grams of styrene oxide and 200 ml of toluene for 30 minutes at room temperature (25° C.) in a single-necked one-liter round-bottomed flask. The flask is placed in a heating mantle and equipped with a water-cooled condenser. The mixture is heated under reflux for three hours producing an oleylamine/styrene oxide adduct.

出典