反応 #4255

反応方程式

cyanuric chloride

dodecyl p-aminobenzoate

HCl

→

1,3,5-Tris-(p-(dodec-1-yloxycarbonyl)-anilino)-s-triazine

溶媒

xylene

反応条件

後処理

1. 1
   洗浄washed twice with saturated sodium bicarbonate solution and once with water
2. 2
   温度cooled to room temperature
3. 3
   ろ過The precipitated crystals were filtered off under suction
4. 4
   その他dried

実験手順

18.5 g of cyanuric chloride and 92 g of dodecyl p-aminobenzoate in 1,000 ml of xylene were heated at 140° C. until HCl gas was no longer evolved. After 8 hours, the reaction solution was cooled to 80° C., washed twice with saturated sodium bicarbonate solution and once with water, and then cooled to room temperature. The precipitated crystals were filtered off under suction and dried.

出典