反応 #42011

反応方程式

ethyl oleate

pentanol

→

pentyl oleate

収率 91.0%

溶媒

ether

反応条件

後処理

1. 1
   温度was refluxed
2. 2
   workup.ADDITIONwas added
3. 3
   ろ過the catalyst was filtered off
4. 4
   濃縮concentrated

実験手順

A mixture containing Catalyst A or B (0.05 g) and ethyl oleate (1.55 g, 5 mmol) and pentanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give pentyl oleate as an oil (1.6 g, 91% yield).

出典