反応 #417934

反応方程式

phenol

3-o-tolylpropanoyl chloride

→

product

収率 93.0%

Phenyl 3-(o-tolyl)propanoate

収率 93.0%

反応条件

後処理

1. 1
   workup.DISTILLATIONdistilled at 127-129° C./0.05 mbar

実験手順

The procedure as described in Example 4a) was repeated with phenol (48 mmol) and 3-o-tolylpropanoyl chloride (55 mmol). The crude product (12.4 g, 97%) was short path distilled at 127-129° C./0.05 mbar to yield 10.6 g (93%) of product as a colourless, semicrystalline oil.

出典