反応 #417926

反応方程式

sodium hydroxide

33

methyl 4-(undec-4Z-enyloxy)benzoate

→

white solid

収率 98.1%

4-(undec-4Z-enyloxy)benzoic acid

収率 98.1%

溶媒

methanol

反応条件

後処理

1. 1
   温度The solution is refluxed for 20 hours
2. 2
   その他After evaporating off the solvent
3. 3
   抽出extracted with DCM

実験手順

550 μL of 1 N sodium hydroxide solution (550 μmol) are added portionwise to 109 mg of 33 (358 μmol) in methanol (4 mL). The solution is refluxed for 20 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 102 mg of a white solid are obtained, i.e. a yield of 98%.

出典