反応 #417924

反応方程式

sodium hydroxide

29

methyl 2-(undec-4Z-enyloxy)benzoate

→

yellow oil

収率 99.5%

2-(undec-4Z-enyloxy)benzoic acid

収率 99.5%

溶媒

methanol

反応条件

後処理

1. 1
   温度The solution is refluxed for 24 hours
2. 2
   その他After evaporating off the solvent
3. 3
   抽出extracted with DCM

実験手順

500 μL of 1 N sodium hydroxide solution (500 μmol) are added portionwise to 80 mg of 29 (263 μmol) in methanol (3 mL). The solution is refluxed for 24 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 76 mg of a yellow oil are obtained, i.e. a yield of 99%.

出典