反応 #417921

反応方程式

acid 22

3-(undecyloxy)benzoic acid

oxalyl chloride

toluene

→

yellow oil

収率 100.1%

3-(undecanyloxy)benzoyl chloride

収率 100.1%

溶媒

DCM

反応条件

後処理

1. 1
   濃縮concentrated

実験手順

1 mL of oxalyl chloride (11.5 mmol) and two drops of anhydrous DMF are added under argon to 93 mg of toluene-dried acid 22 (318 μmol) dissolved in 20 mL of anhydrous DCM. The medium is stirred at room temperature for two hours, and then concentrated to give 99 mg of a yellow oil, i.e. a yield of 99%.

出典