反応 #414899

反応方程式

3-phenyphenol

chlorosulfonyl isocyanate

→

title compound

Sulfamic acid 3-phenylphenyl ester

benzene-acetonitrile

溶媒

toluene

反応条件

実験手順

Using the procedure described in Example 84, the title compound was prepared from 17.0 g (0.010 mole) of 3-phenyphenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 100 ml of toluene to obtain 19.0 g (77%) of white flakes, mp 197°-199° C. (benzene-acetonitrile).

出典