反応 #41355

反応方程式

Sodium periodate

3-phenoxy-1,2-propanediol

→

subtitle compound

収率 100.0%

2-Phenoxyacetaldehyde

収率 100.0%

溶媒

dichloromethane

dichloromethane

反応条件

後処理

1. 1
   ろ過was filtered
2. 2
   濃縮the filtrate was concentrated

実験手順

Sodium periodate (0.65 M in water, 20 mL) was added to a vigorously stirred suspension of silica gel (20 g) in dichloromethane (160 mL), followed by a solution of 3-phenoxy-1,2-propanediol (1.68 g, 10.0 mmol) in dichloromethane (20 mL). After stirring for 10 min the mixture was filtered and the filtrate was concentrated to give the subtitle compound (1.36 g, 100%).

出典