反応 #413221

ord-1a94effe0ac8457cbaabccc480144319

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The product was isolated after chromatography as a low melting point solid

実験手順

Ethyl 2-methyl-2-[4-(6-chloroquinolin-2-yloxy)phenoxy]-propionate (36) was prepared from 2,6-dichloroquinoline and ethyl 2-methyl-2-(4-hydroxyphenoxy)propionate following essentially the same procedure as that described in Example 1. The product was isolated after chromatography as a low melting point solid. Mass spectrum (m/e): 385 (parent ion; 30%); 312 (35%); 271 (100%); 270 (100).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04444584uspto-grants-1984_04