反応 #412324

反応方程式

cyclododecanone

allyl alcohol

di-tert-butyl peroxide

→

2-(3-hydroxypropyl)cyclododecanone

反応条件

後処理

1. 1
   その他From a double-walled vessel made of glass, whose temperature
2. 2
   その他is thermostatically controlled at 100° C.
3. 3
   その他which is fitted with a magnetic stirrer
4. 4
   その他is kept at a temperature of 100° C

実験手順

From a double-walled vessel made of glass, whose temperature is thermostatically controlled at 100° C. and which is fitted with a magnetic stirrer and serves as the storage container for the cyclododecanone, 400 g/h are pumped to a mixing column which is kept at a temperature of 100° C. 21.4 g/h of a mixture of allyl alcohol (12.2 g/h) and di-tert-butyl peroxide (9.2 g/h) are continuously metered into the feedline of the mixing column.

出典