反応 #4073

反応方程式

(S)-2-(6-methoxy-2-naphthyl)-propionic acid

sodium hydroxide

→

sodium (S)-2-(6-methoxy-2-naphthyl)propionate

溶媒

methanol

反応条件

後処理

1. 1
   その他The solvent is evaporated in vacuo
2. 2
   その他followed by precipitation with ether

実験手順

To a solution of 300 mg of (S)-2-(6-methoxy-2-naphthyl)-propionic acid in 5 ml of methanol is added a 1 molar equivalent of sodium hydroxide, in the form of a 0.1N solution. The solvent is evaporated in vacuo and the residue is taken up in 2 ml of methanol, followed by precipitation with ether, to yield crude sodium (S)-2-(6-methoxy-2-naphthyl)propionate.

出典