反応 #40321

ord-36e7a4e2ac1d496fa174c9edc625682a

反応方程式

CCOC(=O)C1CCC(=O)C(Br)C1
3-bromo-4-oxo-cyclohexane carboxylic acid ethyl ester
NC(=S)N=C(N)N
2-imino-4-thiobiuret
CCOC(=O)C1CCc2nc(NC(=N)N)sc2C1
title compound
CCOC(=O)C1CCc2nc(NC(=N)N)sc2C1
2-guanidino-4,5,6,7-tetrahydro-benzothiazole-6-carboxylic acid ethyl ester

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Analogously to the preparation of Example C-01, 3-bromo-4-oxo-cyclohexane carboxylic acid ethyl ester is reacted with 2-imino-4-thiobiuret to form the title compound.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07727979B2uspto-grants-2010_06