反応 #3833
ord-ce2fac42f05a4292a71802d2a5aa59d9
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他This compound was prepared
実験手順
This compound was prepared according to the general method of Example 112 using 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 15 mL of dichloromethane and pyrrolidine (0.63 mL, 7.5 mmol) and triethylamine (1.2 mL, 9 mmol) in 20 mL of dichloromethane, to give 0.75 g of the title compound as a foam, mp 62°-63° C.;