反応 #3814

反応方程式

2,2'-dithiobisbenzoyl chloride

3,5-dichloroaniline

→

title compound

収率 22.5%

2,2'-Dithiobis[N-(3,5-dichlorophenyl)benzamide]

収率 22.5%

溶媒

pyridine

dichloromethane

反応条件

後処理

1. 1
   その他This compound was prepared
2. 2
   その他The crude product was recrystallized from ethanol

実験手順

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 3,5-dichloroaniline (1.87 g, 11.7 mmol) in 15 mL of pyridine. The crude product was recrystallized from ethanol, then ethyl ether to yield 0.78 g of the title compound, mp 235°-236° C.

出典