反応 #366620

反応方程式

15-crown-5

phenylchloroformate

sodium fluoride

→

Phenylfluoroformate

溶媒

acetonitrile

反応条件

後処理

1. 1
   その他Reaction completion

実験手順

To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5(“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).

出典